Invention Patent
- Patent Title: PREPARATION OF 3-AMINOMETHYL-3,5,5-TRIMETHYL -CYCLOHEXYLAMINE
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Application No.: CA2039328Application Date: 1991-03-28
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Publication No.: CA2039328CPublication Date: 2001-11-20
- Inventor: MERGER FRANZ , PRIESTER CLAUS-ULRICH , WITZEL TOM , KOPPENHOEFER GERHARD , HARDER WOLFGANG
- Applicant: MERGER FRANZ , PRIESTER CLAUS-ULRICH , WITZEL TOM , KOPPENHOEFER GERHARD , HARDER WOLFGANG
- Assignee: MERGER FRANZ,PRIESTER CLAUS-ULRICH,WITZEL TOM,KOPPENHOEFER GERHARD,HARDER WOLFGANG
- Current Assignee: MERGER FRANZ,PRIESTER CLAUS-ULRICH,WITZEL TOM,KOPPENHOEFER GERHARD,HARDER WOLFGANG
- Priority: DE4010227 1990-03-30
- Main IPC: B01J21/04
- IPC: B01J21/04 ; B01J21/06 ; B01J23/46 ; B01J27/18 ; C07B61/00 ; C07C209/00 ; C07C209/26 ; C07C209/48 ; C07C209/52 ; C07C211/36 ; C07C211/35
Abstract:
A process for the preparation of 3-aminomethyl-3,5,5-trimethyl-cyclo- hexylamine from 3-cyano-3,5,5-trimethyl-cyclohexanone, wherein the fol- lowing stages are carried out in discrete reaction chambers: a) the 3-cyano-3,5,5-trimethyl-cyclohexanone is reacted in a first reaction chamber with excess ammonia over an acidic metal oxide catalyst at a temperature of from 20.degree. to 150.degree.C and a pressure of from 15 to 500 bar, and b) in a second reaction chamber, the reaction product from stage a) is hydrogenated with hydrogen at a temperature of from 60.degree. to 150.degree.C and a pressure of from 50 to 300 bar in the presence of excess ammonia over a catalyst containing cobalt, nickel, ruthenium, and/or some other noble metal, which catalyst optionally contains a basic component or is supported by neutral or basic supporting material.
Public/Granted literature
- CA2039328A1 PREPARATION OF 3-AMINOMETHYL-3,5,5-TRIMETHYL -CYCLOHEXYLAMINE Public/Granted day:1991-10-01
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