Invention Grant
- Patent Title: Methods for making low remnant free formaldehyde microcapsules and microcapsules made by same
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Application No.: US15240435Application Date: 2016-08-18
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Publication No.: US10005059B2Publication Date: 2018-06-26
- Inventor: Carl M. Lentz , David R. Virgallito , Jerry K. Lawson
- Applicant: Microtek Laboratories, Inc.
- Applicant Address: US OH Dayton
- Assignee: Microtek Laboratories, INC
- Current Assignee: Microtek Laboratories, INC
- Current Assignee Address: US OH Dayton
- Agency: FisherBroyles, LLP
- Agent Susan M. Oiler
- Main IPC: B01J13/18
- IPC: B01J13/18 ; C09K5/06 ; C08G12/32

Abstract:
Methods for producing microcapsules begin by preparing an emulsion of a surfactant, core material, and water, followed by the addition of a crosslinking agent and a melamine formaldehyde prepolymer, which is subsequently polymerized. The crosslinking agent is added before the melamine formaldehyde prepolymer, with a first addition or a second addition of a melamine formaldehyde prepolymer, or is divided for addition with both a first addition and a second addition of melamine formaldehyde prepolymer. The crosslinking agent is a mixture of a reaction product of a cyclic urea (U) and a multifunctional aldehyde (A), and at least one crosslinker selected from the following group: a reaction products of (i) an aminotriazine and at least one aldehyde selected from the group consisting of aliphatic monoaldehydes and multifunctional aliphatic aldehydes, (ii) urea and/or cyclic ureas and formaldehyde, or (iii) phenols and aliphatic monoaldehydes, or from alkoxycarbonylaminotriazines, or multifunctional isocyanates, epoxides, aziridines, and carbodiimides.
Public/Granted literature
- US20170065956A1 METHODS FOR MAKING LOW REMNANT FREE FORMALDEHYDE MICROCAPSULES AND MICROCAPSULES MADE BY SAME Public/Granted day:2017-03-09
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