Invention Grant
- Patent Title: Garnet powder, manufacturing method thereof, solid electrolyte sheet using hot press and manufacturing method thereof
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Application No.: US14716491Application Date: 2015-05-19
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Publication No.: US10008740B2Publication Date: 2018-06-26
- Inventor: Ju Young Sung , Ho Taek Lee , Eun Ji Kwon , Yong Jun Jang , Ji Na Kim
- Applicant: HYUNDAI MOTOR COMPANY
- Applicant Address: KR Seoul
- Assignee: HYUNDAI MOTOR COMPANY
- Current Assignee: HYUNDAI MOTOR COMPANY
- Current Assignee Address: KR Seoul
- Agency: McDermott Will & Emery LLP
- Priority: KR10-2014-0106858 20140818
- Main IPC: H01M10/00
- IPC: H01M10/00 ; H01M10/0562 ; H01M10/0525 ; C01B33/26

Abstract:
The present disclosure relates to garnet powder, a manufacturing method thereof, a solid electrolyte sheet using a hot press, and a manufacturing method thereof. In particular, the present disclosure provides a method for manufacturing Li7La3Zr2O12 (LLZ) garnet powder including preparing a mixture by first dry mixing Li2CO3, La2O3, ZrO2, and Al2O3. The mixture is first calcinated for 5 to 7 hours in a temperature range of 800 to 1000° C. The calcinated mixture is ground to a powder with an average particle size of 1 to 4 μm through dry grinding. A cubic-phased LLZ garnet powder is prepared by second calcinating the ground mixture for 10 to 30 hours in a temperature range of 1100 to 1300° C.
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