Invention Grant
- Patent Title: Nanocomposites containing nonspherical silica nanoparticles, composites, articles, and methods of making same
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Application No.: US14911862Application Date: 2014-08-12
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Publication No.: US10023725B2Publication Date: 2018-07-17
- Inventor: Peter D. Condo , Jeremy O. Swanson , James E. Thorson , William J. Schultz , Kristin L. Thunhorst
- Applicant: 3M INNOVATIVE PROPERTIES COMPANY
- Applicant Address: US MN St. Paul
- Assignee: 3M Innovative Properties Company
- Current Assignee: 3M Innovative Properties Company
- Current Assignee Address: US MN St. Paul
- Agent Adrian L. Pishko
- International Application: PCT/US2014/050659 WO 20140812
- International Announcement: WO2015/069347 WO 20150514
- Main IPC: C08K9/04
- IPC: C08K9/04 ; C09D7/40 ; C08J5/24 ; C09D7/12 ; C08K9/06 ; C08J5/00 ; C08K7/00 ; C08K7/18 ; C08K7/28 ; C08L63/00

Abstract:
A nanocomposite is provided including nonspherical silica nanoparticles dispersed in a curable resin or a curing agent, where the nanocomposite contains less than 2% by weight solvent. A composite is also provided including from about 4 to 70 weight percent of nonspherical silica nanoparticles dispersed in a cured resin, and a filler embedded in the cured resin. Further, a method of preparing a nanoparticle-containing curable resin system is provided including mixing from 10 to 70 weight percent of aggregated silica nanoparticles with a curable resin and optionally a dispersant, a catalyst, a diluent, a surface treatment agent, and/or a curing agent, to form a mixture. The mixture contains less than 2% by weight solvent. The method also includes milling the mixture in an immersion mill containing milling media to form a milled resin system including nonspherical silica nanoparticles dispersed in the curable resin.
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