Invention Grant
- Patent Title: Method for preparing double-sealed-end glycol ether
-
Application No.: US15537928Application Date: 2014-12-22
-
Publication No.: US10040739B2Publication Date: 2018-08-07
- Inventor: Youming Ni , Wenliang Zhu , Hongchao Liu , Yong Liu , Zhongmin Liu , Lina Li , Shiping Liu , Hui Zhou
- Applicant: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- Applicant Address: CN Shahekou Dalian
- Assignee: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- Current Assignee: Dalian Institute of Chemical Physics, Chinese Academy of Sciences
- Current Assignee Address: CN Shahekou Dalian
- Agency: Edwin A. Sisson, Attorney at Law, LLC
- Agent Jeffrey J. Banyas
- International Application: PCT/CN2014/094535 WO 20141222
- International Announcement: WO2016/101104 WO 20160630
- Main IPC: C07C41/14
- IPC: C07C41/14 ; B01J29/65 ; B01J29/40 ; B01J29/18 ; B01J29/70 ; B01J29/08 ; C07C43/10

Abstract:
Disclosed is a method for preparing a double end capped glycol ether, the method comprising: introducing into a reactor a raw material comprising a glycol monoether and a monohydric alcohol ether, and enabling the raw material to contact and react with an acidic molecular sieve catalyst to generate a double end capped glycol ether, a reaction temperature being 50-300° C., a reaction pressure being 0.1-15 MPa, a WHSV of the glycol monoether in the raw material being 0.01-15.0 h−1 , and a mole ratio of the monohydric alcohol ether to the glycol monoether in the raw material being 1-100:1. The method of the present invention enables a long single-pass lifespan of the catalyst and repeated regeneration, has a high yield and selectivity of a target product, low energy consumption during separation of the product, a high economic value of a by-product, and is flexible in production scale and application.
Public/Granted literature
- US20170334818A1 METHOD FOR PREPARING DOUBLE-SEALED-END GLYCOL ETHER Public/Granted day:2017-11-23
Information query