Invention Grant
- Patent Title: Green synthesis of reduced graphene oxide silica nanocomposite using nigella sativa seeds extract
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Application No.: US15151459Application Date: 2016-05-10
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Publication No.: US10052302B2Publication Date: 2018-08-21
- Inventor: Manal Ahmed Gasmelseed Awad , Awatif Ahmed Hendi , Khalid Mustafa Osman Ortashi , Amel Laref
- Applicant: KING SAUD UNIVERSITY
- Applicant Address: SA Riyadh
- Assignee: KING SAUD UNIVERSITY
- Current Assignee: KING SAUD UNIVERSITY
- Current Assignee Address: SA Riyadh
- Agent Richard C. Litman
- Main IPC: A61K31/336
- IPC: A61K31/336 ; A61K9/16 ; A61K33/00

Abstract:
The green synthesis of a reduced graphene oxide (rGO) silica (SiO2) nanocomposite using Nigella sativa seed extract includes mixing a quantity of carbon source in an acid solution while stirring to obtain a solution; adding a first oxidant gradually into the solution to oxidize the soot and obtain a first suspension; stirring the first suspension while maintaining a temperature of the suspension to about 35° C.; adding plant seeds extract to the first suspension while raising the temperature of the suspension to about 60° C.; adding a second oxidant to the suspension to form the reduced graphene oxide nanoparticles; isolating the reduced graphene oxide nanoparticles by centrifugation; suspending the reduced graphene oxide nanoparticles in water; adding a solution comprising tetraethyl orthosilicate (TEOS), concentrated aqueous ammonia solution and a plant seeds extract under ultrasonication; and increasing the temperature to about 90° C. to form reduced graphene oxide-silicon dioxide nanocomposite suspension.
Public/Granted literature
- US20170326097A1 GREEN SYNTHESIS OF REDUCED GRAPHENE OXIDE SILICA NANOCOMPOSITE USING NIGELLA SATIVA SEEDS EXTRACT Public/Granted day:2017-11-16
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