Invention Grant
- Patent Title: Composition and method of manufacturing calcium sulfonate and calcium magnesium sulfonate greases using a delay after addition of facilitating acid
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Application No.: US15593839Application Date: 2017-05-12
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Publication No.: US10087388B2Publication Date: 2018-10-02
- Inventor: J. Andrew Waynick , Joe L. Garza, Jr.
- Applicant: NCH Corporation
- Applicant Address: US TX Irving
- Assignee: NCH CORPORATION
- Current Assignee: NCH CORPORATION
- Current Assignee Address: US TX Irving
- Agency: Ross Barnes LLP
- Agent Robin Barnes
- Main IPC: C10M135/10
- IPC: C10M135/10 ; C10M125/24 ; C10M125/10 ; C10M177/00 ; C10M115/10

Abstract:
A method of making an overbased calcium sulfonate or calcium magnesium sulfonate grease using one or more delay periods between the addition of at least a portion of a facilitating acid, such as DDBSA, and at least a portion of the next subsequently added ingredient. The delay period may be a temperature adjustment delay or a holding delay period. An overbased calcium sulfonate or calcium magnesium sulfonate grease composition comprises 0.5%-5% of a facilitating acid, allows for a reduced amount of overbased calcium sulfonate below 22%, and allows for a reduced amount of calcium hydroxyapatite to provide 10-25% of hydroxide equivalent basicity of the total hydroxide equivalent basicity due to calcium hydroxyapatite and added calcium hydroxide, while maintaining a high dropping point.
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Information query
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