Invention Grant
- Patent Title: Method for producing purified low-substituted hydroxypropyl cellulose
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Application No.: US14079704Application Date: 2013-11-14
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Publication No.: US10174128B2Publication Date: 2019-01-08
- Inventor: Akira Kitamura , Atsuhiko Yonemochi , Mitsuo Narita
- Applicant: Shin-Etsu Chemical Co., Ltd.
- Applicant Address: JP Tokyo
- Assignee: Shin-Etsu Chemical Co., Ltd.
- Current Assignee: Shin-Etsu Chemical Co., Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Alston & Bird LLP
- Priority: JP2012-252191 20121116
- Main IPC: C08B11/02
- IPC: C08B11/02 ; C08B1/08 ; C08B11/08

Abstract:
Provided is a method for producing low-substituted hydroxypropyl cellulose with less yellowing. More specifically, the method for producing purified low-substituted hydroxypropyl cellulose includes the steps of: reacting alkali cellulose and an etherifying agent to obtain a reaction mixture; dispersing the reaction mixture in water containing a portion of acetic acid necessary for neutralizing the total amount of the reaction mixture to neutralize a portion of the reaction mixture, and then completely neutralizing with the remaining acetic acid to cause precipitation, to obtain a slurry containing crude low-substituted hydroxypropyl cellulose; disintegrating a solid component in the slurry through a cutter pump, the solid component containing the crude low-substituted hydroxypropyl cellulose, and discharging the slurry containing the disintegrated solid component; washing the discharged slurry with water to obtain a cake of purified low-substituted hydroxypropyl cellulose; and drying the cake.
Public/Granted literature
- US20140142293A1 Method for Producing Purified Low-Substituted Hydroxypropyl Cellulose Public/Granted day:2014-05-22
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