Invention Grant
- Patent Title: Process and apparatus for vacuum distillation of high-purity magnesium
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Application No.: US15595480Application Date: 2017-05-15
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Publication No.: US10551124B2Publication Date: 2020-02-04
- Inventor: Christian Wegmann , Joerg Loeffler , Peter Uggowitzer , Minh Becker , Heinrich Feichtinger
- Applicant: ETH ZUERICH
- Applicant Address: CH Zurich
- Assignee: ETH Zuerich
- Current Assignee: ETH Zuerich
- Current Assignee Address: CH Zurich
- Agency: Wagenknecht IP Law Group PC
- Priority: EP12000311 20120119
- Main IPC: F27B5/18
- IPC: F27B5/18 ; B01D5/00 ; F27B5/04 ; F27B5/14

Abstract:
A process for producing high-purity magnesium by means of distillation at reduced pressure, characterized in that, the high-purity magnesium condenses in the liquid state, whereby the starting material in the form of a magnesium-containing melt is present together with the upper region of a condensation vessel in the upper region of a retort, whereby the retort consist of a material that releases no volatile impurities into the magnesium steam, whereby the upper region of the retort is brought to a temperature above the boiling point of magnesium, within the limits of two level lines, and is then held constant, such that steam rises from the boiling magnesium-containing metal melt and fills the interior of the upper region of the retort, whereby the steam infiltrating the upper region of the condensation vessel condenses below the lower level line and collects as high-purity melt in the lower region of the condensation vessel, and whereby in order to prevent contaminated melt that drops from the region above the upper level line from reaching the opening of the condensation vessel, this is protected by a cover, which conveys the impure magnesium back again into the melt.
Public/Granted literature
- US20170247776A1 PROCESS AND APPARATUS FOR VACUUM DISTILLATION OF HIGH-PURITY MAGNESIUM Public/Granted day:2017-08-31
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