Invention Grant
- Patent Title: Method for manufacturing furan-2,5-dicarboxylic acid (FDCA) from a salt solution
-
Application No.: US15558244Application Date: 2016-03-17
-
Publication No.: US10577339B2Publication Date: 2020-03-03
- Inventor: Jan Van Krieken , Andre Banier De Haan
- Applicant: PURAC BIOCHEM BV
- Applicant Address: NL Gorinchem
- Assignee: PURAC BIOCHEM BV
- Current Assignee: PURAC BIOCHEM BV
- Current Assignee Address: NL Gorinchem
- Agency: Oliff PLC
- Priority: EP15159401 20150317
- International Application: PCT/EP2016/055820 WO 20160317
- International Announcement: WO2016/146753 WO 20160922
- Main IPC: C07D307/68
- IPC: C07D307/68

Abstract:
A method for manufacturing furan-2,5-dicarboxylic acid (FDCA) by converting a furan-2,5-dicarboxylate salt (MFDC) into FDCA, including the steps of combining an aqueous solution of MFDC with a concentration of at least 5 wt. % with an inorganic acid (HY), to form a reaction mixture including solid FDCA in a concentration of 1-15 wt. % in a salt solution resulting from the cation of furan-2,5-dicarboxylate salt and the anion of the inorganic acid (MY solution), removing solid FDCA from the reaction mixture in a solid/liquid separation step, and providing part of the MY solution resulting from the solid/liquid separation step to the step of combining MFDC with HY. The step of providing part of MY salt solution resulting from the solid/liquid separation step to the step of combining MFDC with HY makes it possible to obtain a stable and economic process which results in an FDCA product with good quality and high yield.
Public/Granted literature
- US20180044312A1 METHOD FOR MANUFACTURING FURAN-2,5-DICARBOXYLIC ACID (FDCA) FROM A SALT SOLUTION Public/Granted day:2018-02-15
Information query