A method of preparing a partially crystalline polycarbonate powder, including: dissolving an amorphous polycarbonate in a halogenated alkane solvent to form a solution; combining the solution with a crystallizing non-solvent that is miscible with the halogenated alkane solvent, under high shear mixing conditions effective to form a partially crystalline polycarbonate precipitate having a D90 particle size of less than 150 micrometers; an average particle diameter of less than or equal to 100 micrometers, or an average particle diameter of 0 to 100 micrometers; and at least 20% crystallinity, or at least 25% crystallinity, or 25 to 35% crystallinity.