Invention Grant
- Patent Title: Polyarylene sulfide production method and polyarylene sulfide production apparatus
-
Application No.: US16096837Application Date: 2018-01-11
-
Publication No.: US10604630B2Publication Date: 2020-03-31
- Inventor: Michihisa Miyahara , Kenji Suzuki , Hiroshi Sakabe
- Applicant: Kureha Corporation
- Applicant Address: JP Tokyo
- Assignee: KUREHA CORPORATION
- Current Assignee: KUREHA CORPORATION
- Current Assignee Address: JP Tokyo
- Agency: Abel Schillinger, LLP
- Priority: JP2017-006747 20170118
- International Application: PCT/JP2018/000477 WO 20180111
- International Announcement: WO2018/135372 WO 20180726
- Main IPC: C08G75/0227
- IPC: C08G75/0227 ; C08G75/0259 ; C08G75/0281

Abstract:
Provided is a PAS production method and a PAS production apparatus wherein, in a gas-liquid system including a gas phase containing water, a dihalo aromatic compound, and hydrogen sulfide and a liquid phase containing a polar organic solvent and PAS, the dihalo aromatic compound and the hydrogen sulfide that can be volatilized at the time of dehydration from the gas phase can be recovered. The PAS production method according to the present invention includes: a condensation step of obtaining a first intermediate gas phase containing a dihalo aromatic compound and hydrogen sulfide and a first intermediate liquid phase containing water, a dihalo aromatic compound, and a sulfur source by condensation from the gas phase in the gas-liquid; a first recovery step of bringing the first intermediate gas phase into contact with a polar organic solvent to obtain a first recovered gas phase containing hydrogen sulfide and a first recovered liquid phase containing a polar organic solvent, a dihalo aromatic compound, and a sulfur source; and a second recovery step of bringing the first recovered gas phase into contact with an alkali metal hydroxide aqueous solution to obtain a second recovered liquid phase containing water, a sulfur source, and an alkali metal hydroxide.
Public/Granted literature
- US20190338075A1 POLYARYLENE SULFIDE PRODUCTION METHOD AND POLYARYLENE SULFIDE PRODUCTION APPARATUS Public/Granted day:2019-11-07
Information query