Invention Grant
- Patent Title: Method for producing 2-acrylamido-2-methylpropane sulphonic acid
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Application No.: US16495207Application Date: 2018-03-19
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Publication No.: US10669231B2Publication Date: 2020-06-02
- Inventor: Cédrick Favero , Johann Kieffer
- Applicant: S.P.C.M. SA
- Applicant Address: FR Andrezieux Boutheon
- Assignee: S.P.C.M. SA
- Current Assignee: S.P.C.M. SA
- Current Assignee Address: FR Andrezieux Boutheon
- Agency: Heslin Rotheberg Farley & Mesiti P.C.
- Priority: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@53b9df15
- International Application: PCT/FR2018/050653 WO 20180319
- International Announcement: WO2018/172677 WO 20180927
- Main IPC: C07C303/20
- IPC: C07C303/20 ; C07C309/15 ; C07C303/44

Abstract:
The present invention relates to a production process for 2-acrylamido-2-methylpropane sulfonic acid including at least the following successive steps: 1) mixing of acrylonitrile with at least one compound contributing SO3 at a temperature included between −80 and 30° C.; 2) placing in contact and mixing isobutylene and the sulfonating mixture with a molar ratio of SO3 to isobutylene included between 0.2:1 and 2:1 and a molar ratio of acrylonitrile to isobutylene included between 3:1 and 60:1 at a temperature included between −40 and 100° C.; 3) solid/liquid separation of the reaction mixture and isolation of the solid particles in the form of a composition 1; 4) mixing composition 1 at the end of step 3) with an aqueous solution A included at a temperature comprised between −20 and 70° C. in order to obtain a suspension 1 of 2-acrylamido-2-methylpropane sulfonic acid crystals; 5) solid/liquid separation of the suspension 1 and isolation of the crystals in form of composition 2.
Public/Granted literature
- US20200024228A1 NEW METHOD FOR PRODUCING 2-ACRYLAMIDO-2-METHYLPROPANE SULPHONIC ACID Public/Granted day:2020-01-23
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