Invention Grant
- Patent Title: Supercritical CO2 cellulose spraydrying
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Application No.: US15762901Application Date: 2016-09-26
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Publication No.: US10669384B2Publication Date: 2020-06-02
- Inventor: Reyes Menendez Gonzalez , Daniela Oana Trambitas , Seda Cantekin , Ian Graveson , Math Jennekens , Saschi Momin
- Applicant: SAPPI Netherlands Services B.V.
- Applicant Address: NL Maastricht
- Assignee: SAPPI Netherlands Services B.V.
- Current Assignee: SAPPI Netherlands Services B.V.
- Current Assignee Address: NL Maastricht
- Agency: Sughrue Mion, PLLC
- Priority: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@5c819e09
- International Application: PCT/EP2016/072826 WO 20160926
- International Announcement: WO2017/051030 WO 20170330
- Main IPC: C08J3/12
- IPC: C08J3/12 ; B01D1/18 ; D21C9/00 ; F26B3/12 ; D21H11/18 ; B01D11/02 ; C08J3/03 ; C08J3/09 ; B82Y40/00

Abstract:
The present invention provides for a process for producing dry, water-dispersible, non-surface modified nanocellulose particles or a powderous composition r comprising said particles comprising the steps of: i. providing a first suspension of non-surface modified cellulose particles in an first aqueous liquid, which aqueous liquid is non-solubilizing for the non-surface modified nanocellulose particles, ii. exchanging substantially all of the first aqueous liquid of the first suspension for a second solvent, which is miscible with the first aqueous liquid and non-solubilizing for the non-surface modified nanocellulose particles, to form a second suspension of non-surface modified nanocellulose particles in said second solvent, iii. contacting a flow of the second suspension of non-surface modified nanocellulose particles with a flow of a fluid in a supercritical or critical state, which fluid in a supercritical or critical state is miscible with the second solvent and non-solvating for the non-surface modified nanocellulose particles under conditions suitable for the transfer of substantially all of the second solvent into the supercritical fluid, iv. removing the second solvent and the fluid in a supercritical or critical state, preferably by controlling pressure and/or temperature, to form the dry, water-dispersible nanocellulose particles, v. collecting the dry, water-dispersible, non-surface modified nanocellulose particles and/or forming the powderous composition comprising said particles.
Public/Granted literature
- US20180282490A1 SUPERCRITICAL CO2 CELLULOSE SPRAYDRYING Public/Granted day:2018-10-04
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