Invention Grant
- Patent Title: Continuous crystallization method under control of multistage membrane
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Application No.: US16314773Application Date: 2017-11-03
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Publication No.: US10675557B2Publication Date: 2020-06-09
- Inventor: Xiaobin Jiang , Guannan Li , Gaohong He , Linghan Tuo , Dapeng Lu , Wu Xiao , Xiangcun Li , Xuemei Wu
- Applicant: Dalian University of Technology
- Applicant Address: CN Dalian, Liaoning
- Assignee: DALIAN UNIVERSITY OF TECHNOLOGY
- Current Assignee: DALIAN UNIVERSITY OF TECHNOLOGY
- Current Assignee Address: CN Dalian, Liaoning
- Agency: Muncy, Geissler, Olds & Lowe, P.C.
- International Application: PCT/CN2017/109249 WO 20171103
- International Announcement: WO2019/084897 WO 20190509
- Main IPC: B01D9/00
- IPC: B01D9/00

Abstract:
The present invention provides a continuous crystallization method under control of the multistage membrane modules, and belongs to the technical field of crystallization engineering. A crystallization solution is added to a crystallizer, and a stirring apparatus and a temperature control apparatus are started. After the system running stability, the loop of crystallization is started. Meanwhile, the coolant or antisolvent feed liquid loop is also started. The crystallization solution can respectively conduct crystal nucleation, growth and ripening in the multistage membrane modules, and then the crystallization solution is transported into a filter device and a drying apparatus to obtain the final crystal products. The desired crystal products can be obtained by the systematical control of the nucleation and crystal growth through the flow and the temperature of the crystallization solution, coolant or antisolvent feed liquid, and the contact time between two liquid phases.
Public/Granted literature
- US20200114277A1 CONTINUOUS CRYSTALLIZATION METHOD UNDER CONTROL OF MULTISTAGE MEMBRANE Public/Granted day:2020-04-16
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