Invention Grant
- Patent Title: Process for the isolation of levulinic acid
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Application No.: US16453188Application Date: 2019-06-26
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Publication No.: US10702792B2Publication Date: 2020-07-07
- Inventor: Aris De Rijke , Rudy Francois Maria Jozef Parton , Donato Santoro
- Applicant: GFBIOCHEMICALS IP ASSETS B.V.
- Applicant Address: NL Geleen
- Assignee: GFBIOCHEMICALS IP ASSETS B.V.
- Current Assignee: GFBIOCHEMICALS IP ASSETS B.V.
- Current Assignee Address: NL Geleen
- Agency: Hudak, Shunk & Farine Co. LPA
- Priority: com.zzzhc.datahub.patent.etl.us.BibliographicData$PriorityClaim@4969ba81
- Main IPC: B01D3/00
- IPC: B01D3/00 ; B01D1/26 ; C07C51/44 ; C07C59/185

Abstract:
A process for the isolation of levulinic acid obtained by acid catalyzed hydrolysis of a C6-carbohydrate-containing feedstock, including the following steps: a) providing a solution 1 comprising at least 5 wt. % of levulinic acid, at least 0.1 wt. % of formic acid and at most 94.9 wt. % of solvent, relative to the total weight of solution 1, b) feeding solution 1 to a first evaporation step to treat solution 1 and to obtain solution 2, comprising at least 25 wt. % of levulinic acid, less than 20 wt. % of solvent and at least 1 wt. % of formic acid, relative to the total weight of solution 2, c) feeding solution 2 to a second evaporation step to treat solution 2 and to obtain solution 3, comprising at least 30 wt. % of levulinic acid and less than 1.0 wt. % of formic acid, relative to the total weight of solution 3, d) feeding solution 3 to a third evaporation step to treat solution 3 and to obtain levulinic acid with a purity of at least 90 wt. % and containing less than 1000 wppm angelica lactone.
Public/Granted literature
- US20190314737A1 PROCESS FOR THE ISOLATION OF LEVULINIC ACID Public/Granted day:2019-10-17
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