Invention Grant
- Patent Title: Method for producing acetic acid
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Application No.: US16334673Application Date: 2018-05-29
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Publication No.: US10752572B2Publication Date: 2020-08-25
- Inventor: Masahiko Shimizu
- Applicant: DAICEL CORPORATION
- Applicant Address: JP Osaka-Shi, Osaka
- Assignee: DAICEL CORPORATION
- Current Assignee: DAICEL CORPORATION
- Current Assignee Address: JP Osaka-Shi, Osaka
- Agency: Birch, Stewart, Kolasch & Birch, LLP
- International Application: PCT/JP2018/020602 WO 20180529
- International Announcement: WO2019/229856 WO 20191205
- Main IPC: C07C51/12
- IPC: C07C51/12 ; C07C51/48 ; C07C51/44

Abstract:
Provided is a method for industrially efficiently producing acetic acid that yields a good potassium permanganate test result, without enormous cost. A light ends column (first distillation column) is operated with a reflux ratio at a specific level or more, a distillation column (crotonaldehyde-removing column) is provided for treating an organic phase of an overhead condensate from the light ends column, and the crotonaldehyde-removing column is operated under such conditions as to meet at least one of conditions (i) to (iii) as follows: (i) a reflux ratio at the distillation column is 0.01 or more; (ii) at the distillation column, the ratio of a crotonaldehyde concentration in a distillate to a crotonaldehyde concentration in a charge liquid is less than 1; and (iii) at the distillation column, the ratio of a crotonaldehyde concentration in bottoms to a crotonaldehyde concentration in the charge liquid is greater than 1.
Public/Granted literature
- US20200123093A1 METHOD FOR PRODUCING ACETIC ACID Public/Granted day:2020-04-23
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