Invention Grant
- Patent Title: Method of synthesizing metal-ascorbic acid crystals
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Application No.: US14963897Application Date: 2015-12-09
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Publication No.: US10774095B2Publication Date: 2020-09-15
- Inventor: Nezar Hassan Khdary , Abdulaziz Almalik
- Applicant: The King Abdulaziz City for Science and Technology
- Applicant Address: SA Riyadh
- Assignee: THE KING ABDULAZIZ CITY FOR SCIENCE AND TECHNOLOGY
- Current Assignee: THE KING ABDULAZIZ CITY FOR SCIENCE AND TECHNOLOGY
- Current Assignee Address: SA Riyadh
- Agency: Dennemeyer & Associates, LLC
- Agent Steven M. Shape
- Main IPC: C07F1/08
- IPC: C07F1/08

Abstract:
The invention provides metal-ascorbic acid crystals and a method for synthesizing the metal-ascorbic acid crystals. The metal in the metal-ascorbic acid crystals is one of copper (Cu), gold (Au) and silver (Ag). The method for synthesizing the metal-ascorbic acid crystals includes sonicating a solution of ascorbic acid and a solvent in dark to obtain a clear solution, wherein the solvent is one of dimethylformamide (DMF) and dimethyl sulfoxide (DMSO). A metal salt is added to the clear solution, wherein the metal salt is one of copper (II) sulfate pentahydrate (CuSO4.5H2O), gold (III)-chloride (AuCl3), and silver sulfate (Ag2SO4). The clear solution is sonicated after adding the metal salt to obtain a reaction mixture. Thereafter, the reaction mixture is heated in dark. The reaction mixture is treated to facilitate solvent extraction of the metal-ascorbic acid. Finally, the metal-ascorbic acid is crystallized.
Public/Granted literature
- US20200231603A1 METHOD OF SYNTHEZING METAL-ASCORBIC ACID CRYSTALS Public/Granted day:2020-07-23
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