Invention Grant
- Patent Title: Method for preparing R—Fe—B sintered magnet
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Application No.: US15710341Application Date: 2017-09-20
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Publication No.: US10937578B2Publication Date: 2021-03-02
- Inventor: Tetsuya Ohashi , Tetsuya Kume , Koichi Hirota , Hajime Nakamura
- Applicant: Shin-Etsu Chemical Co., Ltd.
- Applicant Address: JP Tokyo
- Assignee: Shin-Etsu Chemical Co., Ltd.
- Current Assignee: Shin-Etsu Chemical Co., Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Westerman, Hattori, Daniels & Adrian, LLP
- Priority: JPJP2016-187177 20160926
- Main IPC: H01F1/057
- IPC: H01F1/057 ; H01F41/02 ; B22F3/16 ; B22F3/24 ; C22C38/00

Abstract:
An R—Fe—B base sintered magnet is prepared through the steps of providing an alloy fine powder having a predetermined composition, compression shaping the alloy fine powder in an applied magnetic field into a compact, sintering the compact at a temperature of 900-1,250° C. into a sintered body, cooling the sintered body to 400° C. or below, high-temperature heat treatment including placing a metal, compound or intermetallic compound containing HR which is Dy, Tb and/or Ho, on the surface of the sintered body, heating at a temperature from more than 950° C. to 1,100° C., for causing grain boundary diffusion of HR into the sintered body, and cooling to 400° C. or below, and low-temperature heat treatment including heating at a temperature of 400-600° C. and cooling to 300° C. or below. The sintered magnet produces a high coercivity despite a low content of Dy, Tb and Ho.
Public/Granted literature
- US20180090249A1 METHOD FOR PREPARING R-Fe-B SINTERED MAGNET Public/Granted day:2018-03-29
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