- Patent Title: Method for the manufacture of calcium silicate hydrate used as hardening accelerator in concrete and cement-based materials, calcium silicate hydrate manufactured with said method
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Application No.: US15577268Application Date: 2015-05-29
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Publication No.: US10968108B2Publication Date: 2021-04-06
- Inventor: Jorge Sánchez Dolado , Juan José Gaitero Redondo
- Applicant: FUNDACION TECNALIA RESEARCH & INNOVATION
- Applicant Address: ES Donostia—San Sebastian
- Assignee: FUNDACION TECNALIA RESEARCH & INNOVATION
- Current Assignee: FUNDACION TECNALIA RESEARCH & INNOVATION
- Current Assignee Address: ES Donostia—San Sebastian
- Agency: Squire Patton Boggs (US) LLP
- International Application: PCT/EP2015/061923 WO 20150529
- International Announcement: WO2016/192745 WO 20161208
- Main IPC: C01B33/24
- IPC: C01B33/24 ; C04B22/00 ; C04B14/04 ; C04B40/00 ; C04B40/02

Abstract:
A process for the manufacturing of a slurry containing nucleating agents which comprises reacting at least one source of a Ca containing compound with at least one source of a Si containing compound, in an aqueous media and in the presence of a doping agent selected from the group consisting of P, B, S, and mixtures thereof; wherein: (i) the reaction is carried out at a temperature comprised from 100 to 350° C.; (ii) the total molar ratio Ca/Si is 1.5-2.5, and (iii) the total molar ratio doping agent/Si is 0.01-2; provided that: (a) when the sole doping agent is P, the total molar ratio P/Si is 0.1-2; (b) when the sole doping agent is B, the total molar ratio B/Si is 0.01-2, and (c) when the sole doping agent is S, the total molar ratio S/Si is 0.1-2.
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