Invention Grant
- Patent Title: Method for preparing aliphatic isocyanate
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Application No.: US16642996Application Date: 2018-09-03
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Publication No.: US10975021B2Publication Date: 2021-04-13
- Inventor: Byeong Hyeon Lee , Ju Young Park , Cho Hee Ahn , Sang Hyun Cho
- Applicant: Hanwha Solutions Corporation
- Applicant Address: KR Seoul
- Assignee: Hanwha Solutions Corporation
- Current Assignee: Hanwha Solutions Corporation
- Current Assignee Address: KR Seoul
- Agency: Lex IP Meister, PLLC
- Priority: KR10-2017-0116138 20170911
- International Application: PCT/KR2018/010227 WO 20180903
- International Announcement: WO2019/050236 WO 20190314
- Main IPC: C07C263/10
- IPC: C07C263/10 ; C07C263/04 ; C07C265/08 ; C07C265/12

Abstract:
The present invention relates to a method for preparing an aliphatic isocyanate capable of suppressing the occurrence of side reactions and the production of by-products. The method for preparing an aliphatic isocyanate comprises a step of reacting a salt of an aliphatic amine with phosgene, wherein the reaction step comprises a first reaction step in which phosgene is primarily added and reacted with the salt of an aliphatic amine salt at a temperature of 80 to 100° C., and a second reaction step in which phosgene is secondarily added and reacted with the resultant product of the first reaction step at a temperature of 120 to 160° C., and wherein the amount of the primarily added phosgene is a certain ratio of the total amount of the phosgene.
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