Invention Grant
- Patent Title: Method for preparing reduced titanium powder by multistage deep reduction
-
Application No.: US16319197Application Date: 2018-05-21
-
Publication No.: US11033965B2Publication Date: 2021-06-15
- Inventor: Ting an Zhang , Zhi he Dou , Yan Liu , Guo zhi LV , Qiu yue Zhao , Li ping Niu , Da xue Fu , Wei guang Zhang
- Applicant: Northeastern University
- Applicant Address: CN Shenyang
- Assignee: Northeastern University
- Current Assignee: Northeastern University
- Current Assignee Address: CN Shenyang
- Agency: Muncy, Geissler, Olds & Lowe, P.C.
- Priority: CN201710365974.3 20170523
- International Application: PCT/CN2018/087688 WO 20180521
- International Announcement: WO2018/214849 WO 20181129
- Main IPC: B22F9/20
- IPC: B22F9/20 ; C22B34/12 ; C22B5/18

Abstract:
Provided is a method for preparing a reduced titanium powder by a multistage deep reduction, including the following steps of: uniformly mixing a dried titanium dioxide powder with a magnesium powder to obtain a mixture, adding the mixture in a self-propagating reaction furnace, triggering a self-propagating reaction, obtaining an intermediate product of which low-valence titanium oxides TixO are dispersed in an MgO matrix, leaching the intermediate product with a hydrochloric acid as a leaching solution, performing filtering, washing and vacuum drying to obtain a low-valence titanium oxide TixO precursor, uniformly mixing the low-valence titanium oxide TixO precursor with a calcium powder, performing a pressing to obtain semi-finished products, placing the semi-finished products in a vacuum reduction furnace for a second-time deep reduction, and leaching a deep reduction product with a hydrochloric acid as a leaching solution so as to obtain the reduced titanium powder.
Public/Granted literature
- US20190283139A1 METHOD FOR PREPARING REDUCED TITANUIM POWDER BY MULTISTAGE DEEP REDUCTION Public/Granted day:2019-09-19
Information query