Invention Grant
- Patent Title: Lubricant treatments for free-radical polymerizations
-
Application No.: US16332579Application Date: 2017-09-19
-
Publication No.: US11078441B2Publication Date: 2021-08-03
- Inventor: Sean W. Ewart , Sarat Munjal , Kefu Sun
- Applicant: Dow Global Technologies LLC
- Applicant Address: US MI Midland
- Assignee: Dow Global Technologies LLC
- Current Assignee: Dow Global Technologies LLC
- Current Assignee Address: US MI Midland
- Agency: Dinsmore & Shohl LLP
- International Application: PCT/US2017/052170 WO 20170919
- International Announcement: WO2018/063853 WO 20180405
- Main IPC: C08F10/02
- IPC: C08F10/02 ; C08F110/02 ; C10M175/00 ; C10M129/16 ; C10M133/40 ; C10M135/36 ; C10N40/30

Abstract:
A process to prepare an ethylene-based polymer, said process comprising polymerizing a mixture comprising ethylene, at a pressure greater than, or equal to, 100 MPa, in the presence of at least one free-radical initiator; and in a reactor system comprising at least one reactor and at least one Hyper-compressor, and wherein at least one oil formulation, optionally comprising one or more lubrication agents, is added to the Hyper-compressor; and wherein at least one of the following steps takes place: A) thermally treating the one or more lubrication agents, in an oxygen-free atmosphere, to achieve a peroxide level ≤10 ppm, based on the weight of the lubrication agent(s), and then adding said agent(s) to the oil formulation, prior to adding the oil formulation to the Hyper-compressor; or B) thermally treating the oil formulation, in an oxygen-free atmosphere, to achieve a peroxide level ≤10 ppm, based on the weight of the oil formulation, prior to adding the oil formulation to the Hyper-compressor; C) a combination of A and B.
Public/Granted literature
- US20200277544A1 LUBRICANT TREATMENTS FOR FREE-RADICAL POLYMERIZATIONS Public/Granted day:2020-09-03
Information query