Invention Grant
- Patent Title: Method for producing fibrous cellulose, and fibrous cellulose
-
Application No.: US16814501Application Date: 2020-03-10
-
Publication No.: US11111631B2Publication Date: 2021-09-07
- Inventor: Yuichi Noguchi , Ikue Homma , Yusuke Matsubara
- Applicant: OJI HOLDINGS CORPORATION
- Applicant Address: JP Tokyo
- Assignee: OJI HOLDINGS CORPORATION
- Current Assignee: OJI HOLDINGS CORPORATION
- Current Assignee Address: JP Tokyo
- Agency: Sughrue Mion, PLLC
- Priority: JP2016-071161 20160331
- Main IPC: D21H11/18
- IPC: D21H11/18 ; C08B5/00 ; D21H15/02 ; D21H11/04

Abstract:
It is an object of the present invention to provide a method for producing ultrafine fibrous cellulose, which is capable of efficiently obtaining ultrafine fibrous cellulose having phosphoric acid groups with a high yield. The present invention relates to a method for producing fibrous cellulose having a fiber width of 1000 nm or less, comprising: a (A) of introducing phosphoric acid groups into cellulose fibers to form crosslinked structures via the phosphoric acid groups, thereby obtaining crosslinked phosphorylated cellulose fibers, a (B) of breaking some or all of the crosslinked structures to obtain crosslink-broken phosphorylated cellulose fibers, and a (C) of performing a mechanical treatment on the crosslink-broken phosphorylated cellulose fibers to obtain fibrous cellulose having a fiber width of 1000 nm or less, wherein, in the (A), crosslinked structures in an amount of 0.05 mmol/g or more and 2.0 mmol/g or less are formed, and the (B) is a step of performing the hydrolysis of the crosslinked structures in an aqueous solvent with pH 3 or more.
Public/Granted literature
- US20200208350A1 METHOD FOR PRODUCING FIBROUS CELLULOSE, AND FIBROUS CELLULOSE Public/Granted day:2020-07-02
Information query