Invention Grant
- Patent Title: Process for preparing precipitated silica
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Application No.: US16065533Application Date: 2016-12-22
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Publication No.: US11242260B2Publication Date: 2022-02-08
- Inventor: Rautaray Debabrata , Parida Prabhat Kumar , Lolage Mayura , Phadtare Sumant
- Applicant: Tata Chemicals Limited
- Applicant Address: IN Mumbai
- Assignee: Tata Chemicals Limited
- Current Assignee: Tata Chemicals Limited
- Current Assignee Address: IN Mumbai
- Agency: Frost Brown Todd LLC
- Priority: IN4837/MUM/2015 20151223
- International Application: PCT/IB2016/057918 WO 20161222
- International Announcement: WO2017/109740 WO 20170629
- Main IPC: C01B33/193
- IPC: C01B33/193

Abstract:
A process of preparing precipitated silica is disclosed. Said process comprises of reacting an aqueous solution of a metal silicate with a mineral acid in the presence of a surfactant solution comprising gelatin and C8-C20 sulfosuccinate blend, at a reaction temperature in a range of about 70 to 100° C. with constant stirring such that a reaction mixture having a pH of about 10·0.3 is obtained; optionally, allowing the reaction mixture to age at a temperature in a range of about 70 to 100° C. for a time period in range of 10 to 100 minutes; adjusting the pH of the reaction mixture to about 4, followed by aging said mixture at a temperature in a range of about 70 to 100° C. for a time period in a range of 10 minutes to 2 hours; and recovering the precipitated silica from the reaction mixture.
Information query
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