- Patent Title: Process for purifying a contaminated hydrochloric acid composition
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Application No.: US16466990Application Date: 2017-12-11
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Publication No.: US11352255B2Publication Date: 2022-06-07
- Inventor: Benjamin McKay , Johannes Hendrick Vleeming , Wei Zhao
- Applicant: Avantium Knowledge Centre B.V.
- Applicant Address: NL Amsterdam
- Assignee: Avantium Knowledge Centre B.V.
- Current Assignee: Avantium Knowledge Centre B.V.
- Current Assignee Address: NL Amsterdam
- Agency: Suiter Swantz pc llo
- Priority: NL2017988 20161213
- International Application: PCT/EP2017/082219 WO 20171211
- International Announcement: WO2018/108811 WO 20180621
- Main IPC: C01B7/07
- IPC: C01B7/07 ; C01B7/01 ; C07H1/00

Abstract:
A purified hydrochloric acid composition is prepared from a stream of a contaminated hydrochloric acid composition by a process comprising a distillation treatment, wherein at least a first distillation column is operated at a first pressure and a second distillation column is operated at a second pressure, which second pressure is lower than the first pressure; wherein the contaminated hydrochloric acid composition comprises water, contaminants and hydrochloric acid in a first hydrochloric acid concentration of above the azeotropic composition of hydrochloric acid and water at the first pressure; wherein a part of the stream of the contaminated hydrochloric acid composition is fed into the first distillation column to yield a first bottom product comprising water and hydrochloric acid with a hydrochloric acid concentration below the first hydrochloric acid concentration and a first top product comprising hydrochloric acid in a concentration above the azeotropic hydrochloric acid composition at the first pressure; wherein at least a portion of the first bottom product is passed to the second distillation column; wherein another part of the stream of the contaminated hydrochloric acid composition is fed into the second distillation column to yield a second top product comprising contaminants and water, and a second bottom product comprising water and hydrochloric acid; wherein at least a part of the second bottom product is recycled into the first distillation column; and wherein the first top product is recovered as purified hydrochloric acid composition.
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