Invention Grant
- Patent Title: Nickel powder, method for manufacturing nickel powder, internal electrode paste using nickel powder, and electronic component
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Application No.: US16085148Application Date: 2017-03-14
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Publication No.: US11376658B2Publication Date: 2022-07-05
- Inventor: Junji Ishii , Shingo Murakami , Hiroyuki Tanaka , Takahiro Kamata , Toshiaki Terao , Masaya Yukinobu , Yuji Watanabe , Tsutomu Tanimitsu , Yoshiyuki Kunifusa , Haruo Nishiyama
- Applicant: SUMITOMO METAL MINING CO., LTD. , MURATA MANUFACTURING CO., LTD.
- Applicant Address: JP Tokyo; JP Kyoto
- Assignee: SUMITOMO METAL MINING CO., LTD.,MURATA MANUFACTURING CO., LTD.
- Current Assignee: SUMITOMO METAL MINING CO., LTD.,MURATA MANUFACTURING CO., LTD.
- Current Assignee Address: JP Tokyo; JP Kyoto
- Agency: Katten Muchin Rosenman LLP
- Priority: JPJP2016-056119 20160318
- International Application: PCT/JP2017/010134 WO 20170314
- International Announcement: WO2017/159659 WO 20170921
- Main IPC: B22F1/00
- IPC: B22F1/00 ; B22F1/065 ; B22F9/24 ; H01B1/22 ; H01B1/02 ; C22C19/03 ; B22F1/16

Abstract:
To provide a fine nickel powder for an internal electrode paste of an electronic component, the nickel powder obtained by a wet method and having high crystallinity, excellent sintering characteristics, and heat-shrinking characteristics. The nickel powder is obtained by precipitating nickel by a reduction reaction in a reaction solution including at least water-soluble nickel salt, salt of metal nobler than nickel, hydrazine as a reducing agent, and alkali metal hydroxide as a pH adjusting agent and water; the reaction solution is prepared by mixing a nickel salt solution including the water-soluble nickel salt and the salt of metal nobler than nickel with a mixed reducing agent solution including hydrazine and alkali metal hydroxide; and the hydrazine is additionally added to the reaction solution after a reduction reaction initiates in the reaction solution.
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