Invention Grant
- Patent Title: Method for manufacturing 1,4-bis (4-phenoxybenzoyl)benzene at an elevated temperature
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Application No.: US17291679Application Date: 2019-11-07
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Publication No.: US11434188B2Publication Date: 2022-09-06
- Inventor: Julien Jouanneau , Guillaume Le , Martin Herblot
- Applicant: Arkema France
- Applicant Address: FR Colombes
- Assignee: Arkema France
- Current Assignee: Arkema France
- Current Assignee Address: FR Colombes
- Agency: Buchanan Ingersoll & Rooney P.C.
- Priority: EP18306471 20181109
- International Application: PCT/EP2019/080623 WO 20191107
- International Announcement: WO2020/094818 WO 20200514
- Main IPC: C07C41/00
- IPC: C07C41/00 ; C07C45/46

Abstract:
A method for manufacturing 1,4-bis(4-phenoxybenzoyl)benzene, including: providing a solvent, a Lewis acid, a first reactant and a second reactant, wherein the first reactant and the second reactant are respectively terephthaloyl chloride and diphenyl ether, or reversely; mixing the first reactant in the solvent to make a starting mixture; and, adding the second reactant to the starting mixture; wherein the Lewis acid is mixed, at least partly, to the starting mixture before adding the second reactant to the starting mixture, and/or wherein the Lewis acid is mixed, at least partly, with the second reactant and added together to the starting mixture, and wherein the temperature of the starting mixture is greater than 5° C. during at least part of the step of adding the second reactant to the starting mixture; so as to obtain a product mixture comprising a 1,4-bis(4-phenoxybenzoyl)benzene-Lewis acid complex.
Public/Granted literature
- US20210363088A1 METHOD FOR MANUFACTURING 1,4-BIS (4-PHENOXYBENZOYL)BENZENE AT AN ELEVATED TEMPERATURE Public/Granted day:2021-11-25
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