Invention Grant
- Patent Title: Method for preparing a cross-linked fluorinated polymer film
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Application No.: US16633297Application Date: 2018-07-17
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Publication No.: US11434385B2Publication Date: 2022-09-06
- Inventor: Thierry Lannuzel , Fabrice Domingues Dos Santos , Thibaut Soulestin , Vincent Ladmiral , Bruno Ameduri
- Applicant: ARKEMA FRANCE , CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE , Universite De Montpellier , ECOLE NATIONALE SUPERIEURE DE CHIMIE DE MONTPELLIER
- Applicant Address: FR Colombes; FR Paris; FR Montpellier; FR Montpellier
- Assignee: ARKEMA FRANCE,CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE,Universite De Montpellier,ECOLE NATIONALE SUPERIEURE DE CHIMIE DE MONTPELLIER
- Current Assignee: ARKEMA FRANCE,CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE,Universite De Montpellier,ECOLE NATIONALE SUPERIEURE DE CHIMIE DE MONTPELLIER
- Current Assignee Address: FR Colombes; FR Paris; FR Montpellier; FR Montpellier
- Agency: Buchanan Ingersoll & Rooney P.C.
- Priority: FR1757202 20170728
- International Application: PCT/FR2018/051818 WO 20180717
- International Announcement: WO2019/020906 WO 20190131
- Main IPC: C08F2/46
- IPC: C08F2/46 ; C08F2/50 ; C08G61/04 ; C09D11/106 ; C08F214/24 ; C08K5/00 ; C08K5/06 ; C08K5/07 ; C08K5/10 ; C08K5/17 ; C08K5/36 ; C08K5/521 ; C08L27/16 ; C08L47/00 ; C08L83/08 ; C09D11/101

Abstract:
A process for preparing a crosslinked fluoropolymer film, including the successive steps of: (1) formulating an ink containing: (a) the product of the reaction of triethylamine with at least one fluorinated copolymer obtained by radical copolymerization of monomers including: (i) vinylidene fluoride (VDF), (ii) trifluoroethylene (TrFE), (iii) at least one chlorinated monomer of formula —CXCl═CX1X2 where X, X1 and X2 independently denote H, F or CF3, wherein at most one of X, X1 and X2 denotes CF3; (b) at least one crosslinking agent; (c) at least one photoinitiator; and (d) at least one organic solvent; (2) applying said ink in film form to a substrate; and (3) UV-irradiating said film. Also, the film capable of being obtained according to this process, and also to the uses thereof, in particular in the manufacture of (opto)electronic devices and more particularly in the manufacture of a gate dielectric layer in a field-effect transistor.
Public/Granted literature
- US20200157365A1 METHOD FOR PREPARING A CROSS-LINKED FLUORINATED POLYMER FILM Public/Granted day:2020-05-21
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