- Patent Title: Solvent-stabilized colorimetric detection of amine-based additives
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Application No.: US16900437Application Date: 2020-06-12
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Publication No.: US11560794B2Publication Date: 2023-01-24
- Inventor: Preston Andrew May , Emily Cummings Hart , Jay Paul Deville
- Applicant: Halliburton Energy Services, Inc.
- Applicant Address: US TX Houston
- Assignee: Halliburton Energy Services, Inc.
- Current Assignee: Halliburton Energy Services, Inc.
- Current Assignee Address: US TX Houston
- Agency: Conley Rose, P.C.
- Agent Rodney B. Carroll
- Main IPC: E21B47/135
- IPC: E21B47/135 ; G01N21/78 ; E21B49/08 ; G01N21/77 ; C09K8/035 ; G01N21/31 ; E21B21/00 ; E21B21/06

Abstract:
A method of detecting an amine-based additive in a wellbore servicing fluid (WSF) comprising contacting an aliquot of WSF with an amine detector compound and an aqueous salt solution to form a detection solution; wherein the aqueous salt solution comprises an inorganic salt and organic carboxylate salt; wherein the WSF comprises the amine-based additive; and wherein the detection solution is characterized by at least one absorption peak wavelength in the range of 380-760 nm; detecting an absorption intensity for detection solution at a wavelength within about ±20% of the at least one absorption peak wavelength; comparing the absorption intensity of detection solution at the wavelength within about ±20% of the at least one absorption peak wavelength with a target absorption intensity of amine-based additive to determine the amount of amine-based additive in WSF; and comparing the amount of amine-based additive in WSF with a target amount of amine-based additive.
Public/Granted literature
- US20210388719A1 SOLVENT-STABILIZED COLORIMETRIC DETECTION OF AMINE-BASED ADDITIVES Public/Granted day:2021-12-16
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