Solvent-stabilized colorimetric detection of amine-based additives
Abstract:
A method of detecting an amine-based additive in a wellbore servicing fluid (WSF) comprising contacting an aliquot of WSF with an amine detector compound and an aqueous salt solution to form a detection solution; wherein the aqueous salt solution comprises an inorganic salt and organic carboxylate salt; wherein the WSF comprises the amine-based additive; and wherein the detection solution is characterized by at least one absorption peak wavelength in the range of 380-760 nm; detecting an absorption intensity for detection solution at a wavelength within about ±20% of the at least one absorption peak wavelength; comparing the absorption intensity of detection solution at the wavelength within about ±20% of the at least one absorption peak wavelength with a target absorption intensity of amine-based additive to determine the amount of amine-based additive in WSF; and comparing the amount of amine-based additive in WSF with a target amount of amine-based additive.
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