Invention Grant
- Patent Title: Preparation method for the plant-based nano corrosion inhibition bactericide for oilfield and application thereof
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Application No.: US17863859Application Date: 2022-07-13
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Publication No.: US11624022B2Publication Date: 2023-04-11
- Inventor: Xiankang Zhong , Haonan Li , Zhi Zhang , Junying Hu , Li Zhou , Xi Yuan , Lingjie Li
- Applicant: Southwest Petroleum University
- Applicant Address: CN Chengdu
- Assignee: Southwest Petroleum University
- Current Assignee: Southwest Petroleum University
- Current Assignee Address: CN Chengdu
- Agent Nitin Kaushik
- Priority: CN202110803933.4 20210716
- Main IPC: C09K8/54
- IPC: C09K8/54

Abstract:
The present invention discloses a preparation method for the plant-based nano corrosion inhibition bactericide for oilfield, comprising the following steps: Step 1. Prepare the aloin liquid; Step 2. Stir the carbon nanotube, hydroxyethyl methacrylate and acrylic acid to react for 4 h at a constant temperature of 80° C. to get the carbon nanotube after fiber treatment, namely the modified carbon nanotube; Step 3. Mix the aloin liquid with imidazoline-ammonium-salt, add acetonitrile, and then add modified carbon nanotube, increase the temperature to 95° C. stir and react for 12 hours, and filter after naturally cooling down to room temperature and get the carbon nanotube loaded with bactericide; Step 4. Stir the carbon nanotube loaded with bactericide, diphenylmethane diisocyanate and polycaprolactone to react for 6 hours at a constant temperature of 95° C. and in the reaction process, continuously inject helium to get the target bactericide.
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