Method for preparing high molecular weight furan polyamide
Abstract:
A method for preparing a high molecular weight furan polyamide includes the following steps: 1) charging dimethyl furan dicarboxylate and aliphatic diamine into a reaction container at equal molar weight, and increasing the temperature to 60-120° C. under inert gas; 2) adding a catalyst when the reaction system becomes transparent liquid, increasing the temperature to 140-150° C., and keeping at an atmospheric pressure or a pressure of 41-61 kPa for 0-1 h; and then increasing the temperature to 190-200° C. and reacting for 1-3 h; and 3) depressurizing the system to 3-16 kPa for 0-3 h; and finally, reducing the pressure to 0.003-0.100 KPa for 1-3 h to obtain the high molecular weight furan polyamide.
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