• Patent Title: Method for preparing metal oxide or metal hydroxide nano thin-film material by molten salt method
  • Application No.: US17618879
    Application Date: 2019-09-30
  • Publication No.: US11692258B2
    Publication Date: 2023-07-04
  • Inventor: Yijie GuJinming Wu
  • Applicant: ZHEJIANG UNIVERSITY
  • Applicant Address: CN Hangzhou
  • Assignee: ZHEJIANG UNIVERSITY
  • Current Assignee: ZHEJIANG UNIVERSITY
  • Current Assignee Address: CN Hangzhou
  • Agency: W&G Law Group
  • Priority: CN 1910290149.0 2019.04.11
  • International Application: PCT/CN2019/109582 2019.09.30
  • International Announcement: WO2020/206961A 2020.10.15
  • Date entered country: 2021-12-13
  • Main IPC: C23C2/04
  • IPC: C23C2/04 C23C2/00 C01B13/18 D06M11/36
Method for preparing metal oxide or metal hydroxide nano thin-film material by molten salt method
Abstract:
Provided is a method for preparing a metal oxide or a metal hydroxide nano thin-film material by a molten salt method, which mainly comprises the following steps: heating a low-melting-point salt to a molten state, adding a substrate into the molten salt before or after melting for reaction; adding a metal source and continuing the reaction for a period of time; removing the substrate, cooling the substrate to a room temperature, cleaning and drying the substrate to obtain the metal oxide or metal hydroxide nano thin-film material; wherein, the mass ratio of the low-melting-point salt to the metal source is 100-1.5:1. The metal oxide and metal hydroxide nano-film materials with various nano-morphologies prepared by the method of the present application have morphologies that can be regulated and controlled by the types and proportions of the low-melting-point salts and metal sources.
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