Invention Grant
- Patent Title: Method for preparing sintered NdFeB magnets
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Application No.: US17531809Application Date: 2021-11-22
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Publication No.: US11776719B2Publication Date: 2023-10-03
- Inventor: Xiulei Chen , Zhongjie Peng , Xiaonan Zhu , Zhanji Dong , Kaihong Ding
- Applicant: Yantai Dongxing Magnetic Materials Inc.
- Applicant Address: CN Shandong
- Assignee: Yantai Dongxing Magnetic Materials Inc.
- Current Assignee: Yantai Dongxing Magnetic Materials Inc.
- Current Assignee Address: CN Shandong
- Agent Gang Yu
- Priority: CN 2011313137.4 2020.11.20
- Main IPC: H01F1/057
- IPC: H01F1/057 ; H01F7/02

Abstract:
The present disclosure refers to a method for preparing sintered NdFeB magnets, including:
a) Preparing alloy flakes from a raw material by strip casting, performing a hydrogen decrepitation to produce alloy pieces, pulverization the alloy pieces to an alloy powder, performing molding and orientation, cold isostatic pressing, and getting a green compact;
b) Putting the green compact into a vacuum furnace and performing a first sintering step in 830 to 880° C. for 2 to 10 hours and 5×10−1 Pa or less;
c) Performing a second sintering step while applying a pressure to the green compact achieved by step b), the pressure is 1 MPa to 5 MPa and the sintering temperature is 720 to 850° C. for 15 to 60 minutes, and the temperature of the first sintering step is at least 10° C. higher than that of the second sintering step;
d) Subjecting the sintered magnet of step c) to an annealing treatment.
a) Preparing alloy flakes from a raw material by strip casting, performing a hydrogen decrepitation to produce alloy pieces, pulverization the alloy pieces to an alloy powder, performing molding and orientation, cold isostatic pressing, and getting a green compact;
b) Putting the green compact into a vacuum furnace and performing a first sintering step in 830 to 880° C. for 2 to 10 hours and 5×10−1 Pa or less;
c) Performing a second sintering step while applying a pressure to the green compact achieved by step b), the pressure is 1 MPa to 5 MPa and the sintering temperature is 720 to 850° C. for 15 to 60 minutes, and the temperature of the first sintering step is at least 10° C. higher than that of the second sintering step;
d) Subjecting the sintered magnet of step c) to an annealing treatment.
Public/Granted literature
- US20220165461A1 Method for preparing sintered NdFeB magnets Public/Granted day:2022-05-26
Information query
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