Method for preparing sintered NdFeB magnets
Abstract:
The present disclosure refers to a method for preparing sintered NdFeB magnets, including:



a) Preparing alloy flakes from a raw material by strip casting, performing a hydrogen decrepitation to produce alloy pieces, pulverization the alloy pieces to an alloy powder, performing molding and orientation, cold isostatic pressing, and getting a green compact;
b) Putting the green compact into a vacuum furnace and performing a first sintering step in 830 to 880° C. for 2 to 10 hours and 5×10−1 Pa or less;
c) Performing a second sintering step while applying a pressure to the green compact achieved by step b), the pressure is 1 MPa to 5 MPa and the sintering temperature is 720 to 850° C. for 15 to 60 minutes, and the temperature of the first sintering step is at least 10° C. higher than that of the second sintering step;
d) Subjecting the sintered magnet of step c) to an annealing treatment.
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