Invention Grant
- Patent Title: Methods for graded utilization of fluorine and silicon resources in phosphate ores
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Application No.: US18296356Application Date: 2023-04-05
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Publication No.: US11891344B2Publication Date: 2024-02-06
- Inventor: Xiaowei Quan
- Applicant: CHTEM LIMITED
- Applicant Address: CN Guizhou
- Assignee: CHTEM LIMITED
- Current Assignee: CHTEM LIMITED
- Current Assignee Address: CN Guiyang
- Agency: METIS IP LLC
- Priority: CN 2210413670.0 2022.04.20
- Main IPC: C05B11/08
- IPC: C05B11/08 ; C01B7/19 ; C01B33/107

Abstract:
The present disclosure discloses a method for graded utilization of fluorine and silicon resources in a phosphate ore. While the phosphate ore reacts with sulfuric acid, a fluorine-containing and silicon-containing tail gas is produced. SiO2 and H2SiF6 solution with a high concentration are obtained by concentrating and filtering a solution containing HF and H2SiF6 formed after tail gas is absorbed by water. Crude SiF4 and a solution containing HF and H2SO4 are obtained by extracting, adsorbing, and dehydrating the H2SiF6 solution. SiF4 with a 5N purity is obtained after the crude SiF4 is adsorbed and distilled, at the same time, an impurity-enriched SiF4 is returned to operations of concentration and filtration to react with the solution containing HF and H2SiF6 to generate the H2SiF6 and SiO2. High-purity HF and waste sulfuric acid are obtained after the H2SO4 solution containing HF is separated by steam stripping and distillation.
Public/Granted literature
- US20230339822A1 METHODS FOR GRADED UTILIZATION OF FLUORINE AND SILICON RESOURCES IN PHOSPHATE ORES Public/Granted day:2023-10-26
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