Invention Grant
- Patent Title: Method of producing precursor fiber for carbon fiber and carbon fiber
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Application No.: US17287510Application Date: 2019-10-24
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Publication No.: US11932971B2Publication Date: 2024-03-19
- Inventor: Ayanobu Horinouchi , Fumitaka Watanabe , Yuuki Okishima
- Applicant: Toray Industries, Inc.
- Applicant Address: JP Tokyo
- Assignee: Toray Industries, Inc.
- Current Assignee: Toray Industries, Inc.
- Current Assignee Address: JP Tokyo
- Agency: DLA Piper LLP (US)
- Priority: JP 18202504 2018.10.29 JP 19033752 2019.02.27
- International Application: PCT/JP2019/041603 2019.10.24
- International Announcement: WO2020/090597A 2020.05.07
- Date entered country: 2021-04-21
- Main IPC: D01F9/22
- IPC: D01F9/22 ; D01F6/18 ; D01F9/32

Abstract:
A method of producing a precursor fiber for carbon fiber includes extruding a polyacrylonitrile copolymer solution from a spinneret into the air, immersing it in a coagulation bath liquid stored in a coagulation bath, redirecting traveling of the coagulating fiber bundle by a first guide immersed in the coagulation bath disposed below the spinneret, and pulling it out of the coagulation bath liquid into the air to prepare a coagulated fiber bundle, which is then subjected to at least a washing step in water, stretching step, oil agent applying step, and drying step, wherein the depth-directional coagulation bath immersion length, which means a distance between the starting point of the immersion of the spinning dope solution in the coagulation bath liquid and the first guide immersed in the coagulation bath where traveling of the coagulating fiber bundle is redirected, is 3 to 40 cm.
Public/Granted literature
- US20210395924A1 METHOD OF PRODUCING PRECURSOR FIBER FOR CARBON FIBER AND CARBON FIBER Public/Granted day:2021-12-23
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