Invention Grant
- Patent Title: Method for producing non-core beta silicon carbide fibers
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Application No.: US17620732Application Date: 2020-12-29
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Publication No.: US11959192B2Publication Date: 2024-04-16
- Inventor: Leonid Aleksandrovich Karpyuk , Vladislav Konstantinovich Orlov , Sergey Igorevich Ivanov , Alexey Vladimirovich Glebov , Fyodor Viktorovich Makarov , Roman Gennadyevich Zakharov , Ivan Alexandrovich Dzyubinsky , Alexander Pavlovich Ponomarenko , Dmitry Vladimirovich Zhigalov , Alexander Pavlovich Korolev , Artem Andreevich Vorobyov
- Applicant: BOCHVAR HIGH-TECHNOLOGY RESEARCH INSTITUTE FOR INORGANIC MATERIALS
- Applicant Address: RU Moscow
- Assignee: BOCHVAR HIGH-TECH. RES. INST. FOR INORG. MATERIALS
- Current Assignee: BOCHVAR HIGH-TECH. RES. INST. FOR INORG. MATERIALS
- Current Assignee Address: RU Moscow
- Agency: Craft Chu PLLC
- Agent Andrew W. Chu
- Priority: RU 2020137624 2020.11.17
- International Application: PCT/RU2020/000772 2020.12.29
- International Announcement: WO2022/108475A 2022.05.27
- Date entered country: 2021-12-19
- Main IPC: D01D5/088
- IPC: D01D5/088 ; C01B32/977 ; D01F9/08

Abstract:
The method for producing non-core beta silicon carbide fibers includes four steps. The first step is spinning of multifilament polymeric fiber by melt-extrusion of polycarbosilane. The second step is thermooxidative cross-linking for which the produced spun polymeric fibers are cured in an oxidation furnace at a temperature of 175-250 degrees C. at a heating rate of 3-10 degrees C./h until their weight is increased by 6-15%. The third step is carbonization of the produced cured polymeric fibers with the conversion into the ceramic phase. The fourth step is finishing of the produced beta silicon carbide fiber. The effect of the invention is producing non-core silicon carbide fibers, improving their strength performance, improving resistance to high temperatures and their high creep resistance, stable fiber properties, optimal average diameter of fibers, absence of foreign impurities in the fiber composition.
Public/Granted literature
- US20230026460A1 METHOD FOR PRODUCING NON-CORE BETA SILICON CARBIDE FIBERS Public/Granted day:2023-01-26
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