Invention Grant
- Patent Title: Method and system for preparing xanthate by slurry method
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Application No.: US17005324Application Date: 2020-08-28
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Publication No.: US12054452B2Publication Date: 2024-08-06
- Inventor: Hong Zhong , Xin Ma , Shuai Wang
- Applicant: CENTRAL SOUTH UNIVERSITY
- Applicant Address: CN Hunan
- Assignee: CENTRAL SOUTH UNIVERSITY
- Current Assignee: CENTRAL SOUTH UNIVERSITY
- Current Assignee Address: CN Hunan
- Priority: CN 1810890358.4 2018.08.07
- Main IPC: C07C329/16
- IPC: C07C329/16 ; B03D1/002 ; B03D1/14

Abstract:
A method for preparing xanthate by a slurry method includes steps of: adding a mixture of dichloromethane and carbon disulfide as a reaction solvent in a slurry reactor, and then adding alcohol and caustic alkali to react with carbon disulfide under less than 1 atm to remove heat released by the reaction by evaporating the solvent; performing vacuum distillation after the reaction to remove the solvent and water, so as to obtain the xanthate; transporting the xanthate to a granulation equipment for granulating, and then drying in a drying equipment to obtain a product. The method is performed in a system formed by a reaction equipment, a solvent recovery equipment, the granulation equipment, and the drying equipment, wherein a main equipment of the reaction system is a slurry reactor. The method has advantages of high efficiency, low energy consumption, good safety, environmental friendliness, convenient operation and the like.
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