Invention Grant
- Patent Title: Method for operating a distillation column
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Application No.: US17781413Application Date: 2020-12-09
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Publication No.: US12076670B2Publication Date: 2024-09-03
- Inventor: Klaus Mertens , Sabine Pegel
- Applicant: Covestro Deutschland AG , Covestro Intellectual Property GmbH & Co. KG
- Applicant Address: DE Leverkusen
- Assignee: Covestro Deutschland AG,Covestro Intellectual Property GmbH & Co. KG
- Current Assignee: Covestro Deutschland AG,Covestro Intellectual Property GmbH & Co. KG
- Current Assignee Address: DE Leverkusen; DE Leverkusen
- Agent Donald R. Palladino
- Priority: EP 215603 2019.12.12 EP 210976 2020.12.01
- International Application: PCT/EP2020/085198 2020.12.09
- International Announcement: WO2021/116146A 2021.06.17
- Date entered country: 2022-06-01
- Main IPC: B01D3/42
- IPC: B01D3/42 ; C07C201/16

Abstract:
The present invention relates to a method for continuously operating a distillation column, which is designed to separate a mixture S, which contains essentially a substance A and a substance B, which boils significantly higher than substance A. In the method according to the invention, the reflux ratio is changed according to the feed flow and, at the same time, the energy input by means of the heat-transfer medium is changed proactively (so-called feed-forward control) by accounting for the feed flow by means of feed-forward control. At the same time, the bottom temperature is observed and the control structure is changed if the bottom temperature falls too far when the heat-transfer medium is reduced by means of the feed flow.
Public/Granted literature
- US20230008804A1 METHOD FOR OPERATING A DISTILLATION COLUMN Public/Granted day:2023-01-12
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