Invention Grant
- Patent Title: System and method for preparing epoxy chloropropane
-
Application No.: US18269109Application Date: 2021-12-24
-
Publication No.: US12077516B2Publication Date: 2024-09-03
- Inventor: Liangliang Zhang , Liyang Zhou , Guangwen Chu , Bibo Xia , Jianfeng Chen , Yutu Jiang , Jihong Tong , Baochang Sun , Wei Mao , Yanchun Zheng
- Applicant: QUZHOU JUHUA POLYAMIDE FIBRE LLC. , Beijing University of Chemical Technology , Juhua Group Co., Ltd.
- Applicant Address: CN Zhejiang
- Assignee: QUZHOU JUHUA POLYAMIDE FIBRE LLC.,JUHUA GROUP CO., LTD,BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY
- Current Assignee: QUZHOU JUHUA POLYAMIDE FIBRE LLC.,JUHUA GROUP CO., LTD,BEIJING UNIVERSITY OF CHEMICAL TECHNOLOGY
- Current Assignee Address: CN Quzhou; CN Zhejiang; CN Beijing
- Agency: RANKIN, HILL & CLARK LLP
- Priority: CN 2011564263.7 2020.12.25
- International Application: PCT/CN2021/141200 2021.12.24
- International Announcement: WO2022/135564A 2022.06.30
- Date entered country: 2023-06-22
- Main IPC: C07D303/08
- IPC: C07D303/08

Abstract:
A system and method for preparing epoxy chloropropane is provided in that by coupling three stages of high gravity reactors, the product epoxy chloropropane and water vapor are distilled from a reaction system in form of an azeotrope by adopting a water vapor steam stripping method. Further, by combining the azeotrope with the multiples stages of high gravity reactors, the gas phase mass transfer and the liquid phase mass transfer of the azeotrope are improved aiming at the features of the azeotrope in the reaction system, thus making the overall conversion rate higher. In addition, by combining steam stripping and high gravity, dichloropropanol and alkali solution are rapidly mixed for mass transfer, and the product epoxy chloropropane is rapidly distilled from the reaction system in the form of the azeotrope, such that the reaction proceeds continuously towards the direction of producing epoxy chloropropane, thus significantly improving the conversion rate.
Public/Granted literature
- US20240076277A1 SYSTEM AND METHOD FOR PREPARING EPOXY CHLOROPROPANE Public/Granted day:2024-03-07
Information query