Invention Grant
US06482945B2 Process for producing epsilon-caprolactam and apparatus for the process
失效
用于生产ε-己内酰胺的方法和该方法的装置
- Patent Title: Process for producing epsilon-caprolactam and apparatus for the process
- Patent Title (中): 用于生产ε-己内酰胺的方法和该方法的装置
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Application No.: US09964424Application Date: 2001-09-28
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Publication No.: US06482945B2Publication Date: 2002-11-19
- Inventor: Wolfgang F. Hölderich , Gerd Dahlhoff , Andre Sbresny , Hiroshi Ichihashi
- Applicant: Wolfgang F. Hölderich , Gerd Dahlhoff , Andre Sbresny , Hiroshi Ichihashi
- Priority: JP2000-300264 20000929
- Main IPC: C07D20104
- IPC: C07D20104

Abstract:
A process is provided for producing &egr;-caprolactam from cyclohexanone oxime. The process comprises a evaporation step of a mixture of cyclohexanone oxime and a solvent by introducing the mixture into a fluidized bed in which inert particles is fluidized by an inert gas, the particles having heat enough to evaporate the mixture; and a rearrangement step of cyclohexanone oxime in the evaporated mixture into &egr;-caprolactam by a gas phase Beckmann rearrangement reaction using a solid catalyst, excluding a catalyst consisting of a boric acid or a boron oxide.
Public/Granted literature
- US20020040137A1 Process for producing epsilon-caprolactam and apparatus for the process Public/Granted day:2002-04-04
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