Invention Grant
US06649757B2 Process for producing laurolactam from cyclododecanone 有权
从环十二酮生产十二内酰胺的方法

  • Patent Title: Process for producing laurolactam from cyclododecanone
  • Patent Title (中): 从环十二酮生产十二内酰胺的方法
  • Application No.: US10345548
    Application Date: 2003-01-16
  • Publication No.: US06649757B2
    Publication Date: 2003-11-18
  • Inventor: Nobuyuki KurodaJoji KawaiHideo Shimomura
  • Applicant: Nobuyuki KurodaJoji KawaiHideo Shimomura
  • Priority: JP2002-007549 20020116; JP2002-053903 20020228; JP2002-053931 20020228; JP2002-095024 20020329; JP2002-209935 20020718
  • Main IPC: C07D22502
  • IPC: C07D22502
Process for producing laurolactam from cyclododecanone
Abstract:
Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
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