Invention Grant
- Patent Title: Process for producing laurolactam from cyclododecanone
- Patent Title (中): 从环十二酮生产十二内酰胺的方法
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Application No.: US10345548Application Date: 2003-01-16
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Publication No.: US06649757B2Publication Date: 2003-11-18
- Inventor: Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
- Applicant: Nobuyuki Kuroda , Joji Kawai , Hideo Shimomura
- Priority: JP2002-007549 20020116; JP2002-053903 20020228; JP2002-053931 20020228; JP2002-095024 20020329; JP2002-209935 20020718
- Main IPC: C07D22502
- IPC: C07D22502

Abstract:
Laurolactam having high quality is produced by reacting cyclododecanone with a hydroxylamine salt of a mineral acid, and converting the resultant cyclododecanoneoxime to laurolactam through the Beckmann rearrangement reaction, wherein a content of each of oxygen atom-containing C12 organic compounds, for example, cyclododecenone or epoxycyclododecane, and cycloaliphatic unsaturated C12 hydrocarbon compounds, contained, as an impurity, in the staring cyclododecanone material, is controlled to 1,000 ppm or less.
Public/Granted literature
- US20030139596A1 Process for producing laurolactam from cyclododecanone Public/Granted day:2003-07-24
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