中科微点-全球专利检索

  1. Login
  2. Sign Up
Invention Grant
US07659393B2 Method of preparing cis-8b-methyldecahydro-2a,4a,6a,8a-tetraazacyclopenta[fg]acenaphthylene, cis-decahydro-2a,4a,6a,8a-tetraazacyclopenta[fg]acenaphthylene, cyclene and functionalised cyclenes 失效
顺式-8-甲基十氢化合物2a，4a，6a，8a-四氮杂环戊二烯并[fg]苊烯，顺 - 十氢-2a，4a，6a，8a-四氮杂环戊烯[fg]苊烯，环烯和官能化环烯

Method of preparing cis-8b-methyldecahydro-2a,4a,6a,8a-tetraazacyclopenta[fg]acenaphthylene, cis-decahydro-2a,4a,6a,8a-tetraazacyclopenta[fg]acenaphthylene, cyclene and functionalised cyclenes
Abstract:
A method of preparing cyclene having formula (I) from triethylenetetraamine having formula (VIII) or ethylenediamine having formula (VIII′) includes a series of steps. The first series of steps (I) includes a step A (one-pot preparation of the compound having formula (IIa) from the compound having formula (VIII)), followed by a step B (transforming the compound having formula (IIa) into cyclene having formula (I)). The second series of steps (II) includes a step C (preparing the compound having formula (IIb) from the compound having formula (VIII)), followed by a step D (transforming the compound having formula (IIb) into cylcene having formula (I)). The third series of steps (III) includes a step E involving the onepot preparation of the compound having formula (IIa) from the compound having formula (VIII), followed by a step B involving the transformation of the compound having formula (IIa) into cyclene having formula (I).
Abstract(Chinese):

由具有式（VIII）的三亚乙基四胺或具有式（VIII'）的乙二胺制备具有式（I）的环烯的方法包括一系列步骤。 第一系列步骤（I）包括步骤A（具有式（VIII）化合物的具有式（IIa）的化合物的一锅法制备），然后是步骤B（将具有式（IIa）的化合物转化为 具有式（I）的环烯）。 第二系列步骤（II）包括步骤C（由具有式（VIII）的化合物制备具有式（IIb）的化合物），然后是步骤D（将具有式（IIb）的化合物转化成具有式 一世））。 第三系列步骤（III）包括步骤E，其包括从具有式（VIII）的化合物开始制备具有式（IIa）的化合物的步骤E，随后是涉及将具有式（IIa）的化合物转化为 具有式（I）的环烯烃。

Public/Granted literature
Information query
Espacenet
Patent Agency Ranking
0/0