Invention Grant
- Patent Title: Process for preparing purified terephthalic acid
- Patent Title (中): 制备纯对苯二甲酸的方法
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Application No.: US11793288Application Date: 2005-12-09
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Publication No.: US07692039B2Publication Date: 2010-04-06
- Inventor: Syed Mohammed Azhar Hashmi , Sulaiman Al-Luhaidan
- Applicant: Syed Mohammed Azhar Hashmi , Sulaiman Al-Luhaidan
- Applicant Address: SA Riyadh
- Assignee: Saudi Basic Industries Corporation
- Current Assignee: Saudi Basic Industries Corporation
- Current Assignee Address: SA Riyadh
- Agent Jim Wheelington
- Priority: EP04029615 20041215
- International Application: PCT/IB2005/003722 WO 20051209
- International Announcement: WO2006/085134 WO 20060817
- Main IPC: C07C51/42
- IPC: C07C51/42

Abstract:
The present invention relates to a process for preparing purified terephthalic acid [PTA,], comprising the steps: dissolving crude terephthalic acid [CTA] in an aqueous medium in a reactor; hydrogenating CTA at a temperature of about 260-320° C. and a pressure of about 1100-1300 psig using a hydrogenation catalyst; crystallizing terephthalic acid in the reactor by lowering the temperature of the solution to about 160° C. without evaporation cooling; transferring the content of the reactor to a filtration unit; filtrating the content at a temperature of about 140-160° C. and a pressure of about 40-100 psig, preferably 80-100 psig to obtain a filter cake, washing the filter cake obtained with water having a temperature of about 140-160° C. in the filtration unit; and drying the filter cake.
Public/Granted literature
- US20080275271A1 Process for Preparing Purified Terephthalic Acid Public/Granted day:2008-11-06
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