Invention Grant
- Patent Title: Production of sodium diformate
- Patent Title (中): 二甲酸钠的生产
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Application No.: US12159552Application Date: 2006-12-28
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Publication No.: US07868203B2Publication Date: 2011-01-11
- Inventor: Alexander Hauk , Stefan Gropp , Anna Valeska Lohmann , Robert Heinz
- Applicant: Alexander Hauk , Stefan Gropp , Anna Valeska Lohmann , Robert Heinz
- Applicant Address: DE Ludwigshafen
- Assignee: BASF SE
- Current Assignee: BASF SE
- Current Assignee Address: DE Ludwigshafen
- Agency: Connolly Bove Lodge & Hutz LLP
- Priority: DE102005062931 20051229
- International Application: PCT/EP2006/070246 WO 20061228
- International Announcement: WO2007/074164 WO 20070705
- Main IPC: C07C53/00
- IPC: C07C53/00

Abstract:
The present invention relates to a process for producing a solid sodium diformate preparation having a formic acid content of at least 35% by weight based on the total weight of sodium diformate preparation, in which, at elevated temperature, an aqueous solution (E) is produced which comprises sodium formate and formic acid in a molar ratio of HCOOH:HCOONa of greater than 1.5:1 and which has a molar ratio of HCOOH:H2O of at least 1.1:1, the aqueous solution (E) is brought to crystallization to obtain a solid phase (F) and a mother liquor (G), and the solid phase (F) is separated off from the mother liquor (G), (i) the mother liquor (G) being fed to a distillation apparatus (DV); (ii) the mother liquor (G) in the distillation apparatus (DV) being admixed with a sodium-comprising base (A) to obtain a mixture (B) comprising sodium formate and formic acid; (iii) admixing the mixture (B) obtained from step (ii) with formic acid (D) to obtain the aqueous solution (E); and (iv) excess water (C) essentially being ejected only by withdrawal from the distillation apparatus (DV); and also to the use of a solid sodium diformate preparation obtainable by the inventive process as feed additive for animal feed, in particular for monogastric animal feed and especially for animal feed for hogs and/or poultry.
Public/Granted literature
- US20090061060A1 PRODUCTION OF SODIUM DIFORMATE Public/Granted day:2009-03-05
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