Invention Grant
- Patent Title: Technique for purifying polymer compositions
- Patent Title (中): 聚合物组合物纯化技术
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Application No.: US11304473Application Date: 2005-12-15
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Publication No.: US07994236B2Publication Date: 2011-08-09
- Inventor: James H. Pawlow , William L. Hergenrother
- Applicant: James H. Pawlow , William L. Hergenrother
- Applicant Address: US OH Akron
- Assignee: Firestone Polymers, LLC
- Current Assignee: Firestone Polymers, LLC
- Current Assignee Address: US OH Akron
- Agent Meredith E. Hooker; Arthur M. Reginelli
- Main IPC: C08F6/16
- IPC: C08F6/16

Abstract:
A method for preparing a polymer product, the method comprising polymerizing conjugated diene monomer, optionally together with vinyl aromatic monomer, within a hydrocarbon solvent by employing a lithium-containing initiator, thereby forming a living polymer cement, where about 0.04 to about 0.2 moles of the alkyl lithium initiator per 100 g of the monomer are employed, where the concentration of the monomer within the solvent is about 1 to about 30% by weight, and where the living polymer cement includes a lithium-containing residue, adding a quenching agent to the living polymer cement in an amount sufficient to quench all of the living polymer within the cement, thereby forming a non-living polymer cement, passing the non-living polymer cement through a purification medium, where the purification medium includes alumina, silica, or both, thereby separating at least part of the lithium-containing residue from the polymer cement, collecting the polymer cement after passing the cement through the purification medium, adding an antioxidant, and desolventizing the polymer cement.
Public/Granted literature
- US20070142593A1 Technique for purifying polymer compositions Public/Granted day:2007-06-21
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