Invention Grant
- Patent Title: Process for producing urethane (meth)acrylate
- Patent Title (中): 制备聚氨酯(甲基)丙烯酸酯的方法
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Application No.: US12922207Application Date: 2009-03-12
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Publication No.: US08148567B2Publication Date: 2012-04-03
- Inventor: Fumihiko Ishiyama , Takeshi Hizawa , Hideki Watanabe
- Applicant: Fumihiko Ishiyama , Takeshi Hizawa , Hideki Watanabe
- Applicant Address: JP Tokyo
- Assignee: DIC Corporation
- Current Assignee: DIC Corporation
- Current Assignee Address: JP Tokyo
- Agency: Edwards Wildman Palmer LLP
- Agent James E. Armstrong, IV; Junko Harada
- Priority: JP2008-065709 20080314
- International Application: PCT/JP2009/054732 WO 20090312
- International Announcement: WO2009/113608 WO 20090917
- Main IPC: C07C269/00
- IPC: C07C269/00

Abstract:
An object of the present invention is to provide a process for producing a urethane (meth)acrylate safely with good productivity, and for achieving the object, the invention provides a process for continuously producing a urethane (meth)acrylate, containing causing a mixed liquid of a compound (A) having a hydroxyl group and a (meth)acryloyl group and a compound (B) having an isocyanate group to pass continuously and densely through a tubular microchannel formed in a heat-conducting reaction device, and reacting the hydroxyl group of the compound (A) with the isocyanate group of the compound (B), in which the tubular microchannel in the reaction device has a space size making a fluid cross-sectional area, through which the mixed liquid passes densely, of from 0.1 to 4.0 mm2, and the process contains heating the heat-conducting reaction device to a temperature of from 100 to 250° C., reacting the mixed liquid to provide a Reynolds number of a reaction liquid passing through the tubular microchannel in a range of from 0.2 to 300, and after completing reaction, cooling continuously a reaction product discharged from the heat-conducting reaction device.
Public/Granted literature
- US20110087041A1 PROCESS FOR PRODUCING URETHANE (METHA)ACRYLATE Public/Granted day:2011-04-14
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