Invention Grant
- Patent Title: Method of producing pre-oxidation fiber and carbon fiber
- Patent Title (中): 生产预氧化纤维和碳纤维的方法
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Application No.: US12747386Application Date: 2008-12-10
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Publication No.: US08236273B2Publication Date: 2012-08-07
- Inventor: Taro Oyama , Rie Kawahito , Hiroshi Kimura
- Applicant: Taro Oyama , Rie Kawahito , Hiroshi Kimura
- Applicant Address: JP Tokyo
- Assignee: Toho Tenax Co., Ltd.
- Current Assignee: Toho Tenax Co., Ltd.
- Current Assignee Address: JP Tokyo
- Agency: Sughrue Mion, PLLC
- Priority: JP2007-341567 20071230
- International Application: PCT/JP2008/072381 WO 20081210
- International Announcement: WO2009/084390 WO 20090709
- Main IPC: D01F9/12
- IPC: D01F9/12

Abstract:
There is disclosed a method of producing a pre-oxidation fiber in the production of the pre-oxidation fiber by subjecting a polyacrylic precursor fiber to pre-oxidation processing in an oxidizing atmosphere, including shrinking the precursor fiber as a pretreatment of pre-oxidation at a load of 0.58 g/tex or less in the temperature range of 220 to 260° C. under conditions in which the degree of cyclization (I1620/I2240) of the precursor fiber measured by a Fourier transform infrared spectrophotometer (FT-IR) does not exceed 7%, initially-drawing the precursor fiber at a load of 2.7 to 3.5 g/tex in an oxidizing atmosphere at 230 to 260° C. in the ranges of the degree of cyclization of not exceeding 27% and of the density of not exceeding 1.2 g/cm3, and then subjecting the pre-oxidation fiber to pre-oxidation treatment. A carbon fiber of high strength and high elasticity that is appropriate for composite materials that exhibit high composite performance is obtained by continuously subjecting this pre-oxidation fiber to carbonization treatment.
Public/Granted literature
- US20100260658A1 METHOD OF PRODUCING PRE-OXIDATION FIBER AND CARBON FIBER Public/Granted day:2010-10-14
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