Invention Grant
- Patent Title: Process of making polyacrylonitrile fibers
- Patent Title (中): 制备聚丙烯腈纤维的方法
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Application No.: US12585304Application Date: 2009-09-10
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Publication No.: US08372323B2Publication Date: 2013-02-12
- Inventor: W. Kenneth Wilkinson
- Applicant: W. Kenneth Wilkinson
- Applicant Address: US VA Fairfax
- Assignee: International Fibers, Ltd.
- Current Assignee: International Fibers, Ltd.
- Current Assignee Address: US VA Fairfax
- Main IPC: D01D5/06
- IPC: D01D5/06 ; D01D5/16 ; D01D10/02 ; D01F6/40 ; D02G3/02

Abstract:
A process for preparing a PANOX fiber comprising: obtaining an acrylonitrile copolymer, wherein the copolymer contains at least about 2% by weight itaconic acid comonomer; forming a spin dope from the copolymer; wet spinning the spin dope to obtain gelled filaments; contacting the gelled filaments with ammonia activator in an aqueous imbibation bath; bundling the gelled filaments to obtain a fiber; removing solvent from the fiber; drawing the fiber; densifying the fiber by heating the fiber up to about 400 degrees C. for a time of about 15 minutes in a rapid densification zone; and withdrawing a PANOX fiber from the densification zone.
Public/Granted literature
- US20110059314A1 Process and apparatus for preparing superior carbon fiber Public/Granted day:2011-03-10
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