Invention Grant
- Patent Title: Method for producing liquid crystal polyester
- Patent Title (中): 液晶聚酯的制造方法
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Application No.: US13429954Application Date: 2012-03-26
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Publication No.: US08383759B2Publication Date: 2013-02-26
- Inventor: Shinji Ohtomo , Tadashi Fukunaka , Yi Zhang
- Applicant: Shinji Ohtomo , Tadashi Fukunaka , Yi Zhang
- Applicant Address: JP Tokyo
- Assignee: Sumitomo Chemical Company, Limited
- Current Assignee: Sumitomo Chemical Company, Limited
- Current Assignee Address: JP Tokyo
- Agency: Panitch Schwarze Belisario & Nadel LLP
- Priority: JP2011-072010 20110329
- Main IPC: C08G63/18
- IPC: C08G63/18 ; C08G63/52

Abstract:
A method is provided for producing a liquid crystal polyester including: (1) polycondensing a mixture of a compound of formula (I) with a compound of formula (II) in a polymerization tank at 260 to 350° C. to form a prepolymer, wherein a ratio of by-products to be distilled off to the theoretical amount of by-products formed when the compound of formula (I) is polycondensed with the compound of formula (II) in a stoichiometric relation is 95% or more; (2) continuously discharging the prepolymer from the polymerization tank in a molten state, solidifying the prepolymer while transferring, and continuously grinding the solidified prepolymer by a grinder provided downstream in a transfer direction to produce prepolymer particles; and (3) heat-treating the prepolymer particles in their solid state under an inert gas atmosphere, thereby subjecting them to solid phase polymerization.
Public/Granted literature
- US20120253003A1 METHOD FOR PRODUCING LIQUID CRYSTAL POLYESTER Public/Granted day:2012-10-04
Information query
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